Quantitative Analysis Of Dicyclohexylamine And Impurities

HPLC-ELSD was used to study the quantitative analysis of dicyclohexylamine. The recoveries were 98.2%-102.45% with RSD of 8.39-9.3%. In addition, HECEDA was used to study the simultaneous quantitative analysis of aminophenol and aniline. The limits of quantification were 1 and 0.5ng, and the linear ranges were 0-40 mg/L and 0-20 mg/L, respectively. The accuracy and precision of the analytical method can meet the requirements of product quality testing.


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At present, there are few reports on the quantitative analysis of dicyclohexylamine and impurities, so it is necessary to study them separately accurate quantitative analysis method. 

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Since dicyclohexylamine has no ultraviolet absorption, the quantitative analysis method of dicyclohexylamine by high performance liquid chromatography evaporative light scattering detector was studied. 


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